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HRID436692

反应详情

EQUATION

反应方程式

HRID 436692 的结构方程式

REACTANTS

反应物

2
结构：CSC(SC)=C(C#N)C#N
HCID99229

Propanedinitrile, [bis(methylthio)methylene]-

C6H6N2S2

结构：CSC(SC)=C(C#N)C(N)=O
HCID2747746

2-cyano-3,3-bis(methylthio)acrylamide

C6H8N2OS2

PRODUCTS

生成物

1
结构：N#CC(C(N)=O)=C1Nc2ccccc2O1
HCID70622182

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The procedure described in Example 1 is repeated using, instead of 3,3-bis(methylthio)-2-cyanoacrylonitrile, an equivalent amount of 3,3-bis(methylthio)-2-cyanoacrylamide and holding the mixture under reflux for 12 hours to obtain 2-benzoxazolinylidene-cyanoacetic acid amide of melting point 220°-222° C. (dec.) (from methanol).

WORKUP

后处理

  1. temperatureunder reflux for 12 hours