HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl Alcohol → HCID 70622289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-(Bis(methylsulfanyl)methylidene)propanedinitrile | HCID 99229 | — |
| Reactant | HCID 54525267 | HCID 54525267 | — |
| Product | HCID 70622289 | HCID 70622289 | — |
Reaction Steps
The procedure described in Example 1 is repeated using, instead of 3,3-bis(methylthio)-2-cyanoacrylonitrile, an equivalent amount of 3,3-bis(methylthio)-2-cyanoacrylic acid allyl ester in 100 ml. of allyl alcohol and holding the mixture under reflux for 7 hours to obtain 2-benzoxazolinylidene-cyanoacetic acid allyl ester of melting point 181°-183° C. (from ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028089 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-216773d60f3b4a949228b26ac7705a9e |
| Source note | uspto-grants-1977_06 |