HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20369400, compound → HCID 73793283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20369400 | HCID 20369400 | — |
| Reactant | HCID 21431388 | HCID 21431388 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 73793283 | HCID 73793283 | — |
Reaction Steps
In the manner given in Example 1, 7-fluoro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine in tetrahydrofuran can be treated with 3-chloro-1-hydroxy-2-butanone under nitrogen to give 7-fluoro-2-[[2-chloro-1-(hydroxymethyl)propylidene]hydrazino]-5-phenyl-3H-1,4-benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028356 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-ab9bff7196604d679de741c8a23fe62c |
| Source note | uspto-grants-1977_06 |