HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dichlorobutan-2-one → HCID 53641671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dichlorobutan-2-one | HCID 85563 | — |
| Reactant | HCID 22768402 | HCID 22768402 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53641671 | HCID 53641671 | — |
Reaction Steps
In the manner given in Example 1, 7-(trifluoromethyl)-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine in tetrahydrofuran can be treated with 1,4-dichloro-2-butanone under nitrogen to give 7-(trifluoromethyl)-2-[[2-chloro-1-(2-chloroethyl)ethylidene]hydrazino]-5-phenyl-3H-1,4-benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028356 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-917ba5a4291a4a1fa3ec7dfb646e2429 |
| Source note | uspto-grants-1977_06 |