Methanethiol → HCID 21431585, compound

HRID 436821Notes

Reaction equation

HRID 436821 reaction equation
[C:1]([C:5]1[CH:9]=[C:8]([N:10]=[C:11]=[O:12])[O:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH3:13][SH:14]>>[C:1]([C:5]1[CH:9]=[C:8]([NH:10][C:11](=[O:12])[S:14][CH3:13])[O:7][N:6]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 878MethanethiolHCID 13292893HCID 13292893, compound

Product 1

HCID 21431585HCID 21431585, compound

Procedure

Using 3-t-butyl-5-isoxazolyl isocyanate and methyl mercaptan, the reaction is effected as in Synthetic Example 17, whereby S-methyl 3-t-butyl-5-isoxazolylthiocarbamate is obtained as crystals melting at 104.0° to 105.5° C.

Sources & evidence

ORD record
ord-a514ef63e9bd4b149461cedebdee8026
Source dataset
uspto-grants-1977_06
Patent number
US04028376

Reaction notes

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