HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → O-Benzyl Glycine Hydroxamic Acid Trifluoroacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-[(tert-Butoxy)carbonylamino]-N-(phenylmethoxy)acetamide | HCID 14694702 | — |
| Product | O-Benzyl Glycine Hydroxamic Acid Trifluoroacetate | HCID 86734842 | — |
Reaction Steps
T-Butyloxycarbonyl-O-benzyl glycine hydroxamic acid [(17.5 g, 62.5 mMol) see Step A] was dissolved in trifluoroacetic acid (25 ml), stirred at room temperature thirty minutes, and ether (200 ml) added. The product was filtered and dried to yield: 9.0 g, m.p. 122°-124°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028401 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-96cd1edef6b048ce88592ae00f6774ea |
| Source note | uspto-grants-1977_06 |