HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 21431781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Cyclobutyl(4-methylphenyl)methanone | HCID 316820 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 21431781 | HCID 21431781 | — |
Reaction Steps
Cyclobutyl p-tolyl ketone (30 g) and N-bromosuccinimide (31 g) in carbon tetrachloride (200 ml) were irradiated and heated under reflux with a tungsten lamp for 1.5 hours, and cooled. The mixture was filtered and the filtrate was evaporated. The residue was distilled under reduced pressure and the fraction b.p. 120°-125°/0.015 mm was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028404 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-c57fb131a4964a3ab66436218945fbe4 |
| Source note | uspto-grants-1977_06 |