HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethylphenol → HCID 131710812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethylphenol | HCID 7771 | — |
| Reactant | Aluminum isopropoxide | HCID 11143 | — |
| Reactant | Zirconium butoxide | HCID 160560 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 131710812 | HCID 131710812 | — |
Reaction Steps
instead of aluminum isopropoxide, 0.8 g of tetrabutyl zirconate (as a 30% solution in xylene) is added to the 2,4-dimethylphenol. Butyl alcohol and xylene are removed with heat and vacuum to yield zirconium 2,4-dimethylphenoxide, which upon addition of toluene and divinylbenzene and reaction in accordance with part A of Example I, functions as an alkylation catalyst, yielding a similar yield of the same styryl monomer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028342 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-987bc7261ff44ad9ae2a306940dc66a0 |
| Source note | uspto-grants-1977_06 |