HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 12665791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 12665764 | HCID 12665764 | — |
| Product | HCID 12665791 | HCID 12665791 | — |
Reaction Steps
To an aqueous solution of 3-chloro-1,2-dimethyl-5-phenylpyrazolium methyl sulfate is added a saturated aqueous solution of sodium iodide at 5° C. A copious precipitate is formed and filtered off. The solid is dissolved in methylene chloride and precipitated with diethyl ether to yield almost white crystals mp 162° C. to 164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029492 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-9f44a8c0f49a493c889fe5d260a18a7d |
| Source note | uspto-grants-1977_06 |