HRID437014

反应详情

EQUATION

反应方程式

HRID 437014 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

In 100 parts of acetone containing 40 wt. % of water, 10 parts of potassium p-styrenesulfonate and 10 parts of ammonium sulfate were charged. The mixture was stirred at 60° C. for 30 minutes. After cooling to 30° C., the reaction was filtered and the filtrate was condensed and dried to obtain 9.0 parts of ammonium p-styrenesulfonate. Analysis showed that only 0.15 wt. % of K and 0.01 of SO4 were included in the product.

WORKUP

后处理

  1. temperatureAfter cooling to 30° C.
  2. filtrationthe reaction was filtered
  3. customcondensed
  4. customdried