HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylallylamine → Allyl n-butoxymethyl dimethylammonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylallylamine | HCID 75082 | — |
| Reactant | 1-(Chloromethoxy)butane | HCID 11105357 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Allyl n-butoxymethyl dimethylammonium chloride | HCID 21429949 | — |
Reaction Steps
24.7 grams of chloromethyl butyl ether was added to 17 grams of allyl dimethylamine in 32 grams of ethyl acetate. The reaction was highly exothermic and two layers formed very rapidly. Stirring was continued at 25° C. for 24 hours, after which the solvent was removed by vacuum. Chloride analysis of the rather viscous liquid product indicated 91% of theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029658 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-555e2f750b504c65a2b53b679bcae8c9 |
| Source note | uspto-grants-1977_06 |