HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylbenzylamine → Benzenemethanaminium, N,N-dimethyl-N-2-propenyl-, chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylbenzylamine | HCID 7681 | — |
| Reactant | Allyl chloride | HCID 7850 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Benzenemethanaminium, N,N-dimethyl-N-2-propenyl-, chloride | HCID 11287299 | — |
Reaction Steps
27 grams of dimethylbenzyl amine was added to 15.4 grams of allyl chloride in 42.4 grams of ethyl acetate. The reaction was endothermic, with a crystalline product forming within 5 minutes. After 7 days standing at 25° C., the white solid was filtered, washed, and dried. The chloride content of the quaternary halide was 95.5% of theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029658 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-1cf8b5c5ceb74091957020993cdcbd2d |
| Source note | uspto-grants-1977_06 |