Allyl chloride → HCID 14327232, compound

HRID 437034Notes

Reaction equation

HRID 437034 reaction equation
[CH3:1][N:2]([CH2:4][CH2:5][OH:6])[CH3:3].[CH2:7]([Cl:10])[CH:8]=[CH2:9]>O>[Cl-:10].[CH2:7]([N+:2]([CH3:3])([CH3:1])[CH2:4][CH2:5][OH:6])[CH:8]=[CH2:9]

Participants

4

Reactant 2

HCID 7850Allyl chlorideHCID 79022-(Dimethylamino)ethanol

Product 1

HCID 14327232HCID 14327232, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

89 grams of N-dimethylaminoethanol were dissolved in 244.7 grams of water, to which 76.5 grams of allyl chloride were added slowly and with cooling, keeping the temperature below 35° C. The reaction was essentially complete within one hour. A clear solution was obtained.

Workup

  1. additionwere added slowly
  2. temperaturewith cooling
  3. customthe temperature below 35° C
  4. customA clear solution was obtained

Sources & evidence

ORD record
ord-d3597643cdc94a21958771beb7efaa2d
Source dataset
uspto-grants-1977_06
Patent number
US04029658

Reaction notes

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