HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-AlaAlaPro-OBzl → Boc-ala-ala-pro-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-AlaAlaPro-OBzl | HCID 15289361 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Boc-ala-ala-pro-OH | HCID 11902955 | — |
Reaction Steps
A solution of 0.015 moles of t-butyloxycarbonylalanylalanylproline benzyl ester in 50 ml of methanol is reduced with hydrogen at 40 lbs pressure in the presence of 1 gm of 10% Pd/C. The reaction mixture is filtered and concentrated in vacuo to give t-butyloxycarbonylalanylalanylproline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029772 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-474a424d05a1456987a1539b0b3ee539 |
| Source note | uspto-grants-1977_06 |