HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 53865690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 4-Chloro-3-[(cyclohexylmethylamino)sulfonyl]benzoic acid | HCID 43078258 | — |
| Product | HCID 53865690 | HCID 53865690 | — |
Reaction Steps
The reaction was carried out in a manner analogous to that of Example 31, using 33 g of 4-chloro-3-(N-methylcyclohexylaminosulfonyl)-benzoic acid and 30 g of N-methylpiperazine. The moist crude product, which had been washed with water, was freed from by-products by boiling with methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029787 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-09156b18fbd34cb9948e0ef9cfd9d4b5 |
| Source note | uspto-grants-1977_06 |