1H-Indene, 3-(3-bromopropyl)- → HCID 21430578, compound

HRID 437222Notes

Reaction equation

HRID 437222 reaction equation
[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([CH2:10][CH2:11][N:12]2[CH2:17][CH2:16][CH:15]([NH:18][C:19](=[O:26])[C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[CH2:14][CH2:13]2)=[CH:2]1.Br[CH2:28]CCC1C2C(=CC=CC=2)CC=1>>[CH2:28]1[C:8]2[C:9](=[CH:1][CH:2]=[CH:6][CH:7]=2)[C:4]([CH2:3][CH2:10][CH2:11][N:12]2[CH2:13][CH2:14][CH:15]([NH:18][C:19](=[O:26])[C:20]3[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=3)[CH2:16][CH2:17]2)=[CH:5]1

Participants

3

Reactant 2

HCID 105378211H-Indene, 3-(3-bromopropyl)-HCID 21430607HCID 21430607, compound

Product 1

HCID 21430578HCID 21430578, compound

Procedure

Prepared in a similar manner to the compound of Example 14 but using 3-(3-bromopropyl)indene in place of 3-(2-bromoethyl)indene. The title compound crystallised from isopropanol, m.p. 157°-9° C. (Found: C, 79.8; H, 8.1. N, 7.7. C24H28N2O requires C, 80.0; H, 7.8; N, 7.8%).

Workup

  1. customThe title compound crystallised from isopropanol, m.p. 157°-9° C. (Found: C, 79.8; H, 8.1. N, 7.7. C24H28N2O requires C, 80.0; H, 7.8; N, 7.8%)

Sources & evidence

ORD record
ord-f105bdbeac59440b9b3dc6c766417a32
Source dataset
uspto-grants-1977_06
Patent number
US04029801

Reaction notes

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