HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 21427792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 3-Cyclohexene-1-propanal, beta,4-dimethyl- | HCID 110923 | — |
| Product | HCID 21427792 | HCID 21427792 | — |
Reaction Steps
The procedure of Example 1 was followed using 50g (0.3 mole) of 3-(4-methyl-3-cyclohexenyl)butyraldehyde and 24g (0.33 mole) of pyrrolidine. Obtained following distillation was 48.5g of pure N-[3 . . . butyl]pyrrolidine as a clear, colorless liquid: bp 106°-108° (0.2mm) ir (τ max. film 3.5 (s), 6.9 (s), 7.3 (s), 8.7 (s), 12.5 (m) microns; nmr (δ, CDCl3) 5.36 (m, 1H), 2.45 (m, 6H), 2.1 to 0.8 (m, 20H) ppm; ms (molecular ion) 221.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04030908 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-54346f27d05b47c8a201e8486ce3a959 |
| Source note | uspto-grants-1977_06 |