HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetyl-2-(4-benzalaminophenyl)hydrazine → N'-[4-(benzylamino)phenyl]acetohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetyl-2-(4-benzalaminophenyl)hydrazine | HCID 21427836 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N'-[4-(benzylamino)phenyl]acetohydrazide | HCID 21427829 | — |
Reaction Steps
1-Acetyl-2-(4-benzalaminophenyl)hydrazine (5.1 g, 0.02 mole) and platinum oxide (catalytic amount) were suspended in ethanol (200 ml) in a Parr shaker bottle. The reaction mixture was hydrogenated at room temperature until hydrogen uptake ceased. The reaction mixture was filtered and the solvent was evaporated from the filtrate leaving a white crystalline powder. Yield 4.7 g (92%), m.p. 118°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04030925 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-434ba318515c4384a8edd49ad841bd82 |
| Source note | uspto-grants-1977_06 |