HCID 54356452, compound → HCID 54711095, compound

HRID 437366Notes

Reaction equation

HRID 437366 reaction equation
[CH2:1]([N:4]([C:8]1[CH2:13][CH2:12][CH2:11][CH2:10][C:9]=1[C:14]([OH:16])=O)[C:5](=[O:7])[CH3:6])[CH2:2][CH3:3]>CCO>[OH:16][C:14]1[C:9]2[CH2:10][CH2:11][CH2:12][CH2:13][C:8]=2[N:4]([CH2:1][CH2:2][CH3:3])[C:5](=[O:7])[CH:6]=1

Participants

3

Reactant 1

HCID 54356452HCID 54356452, compound

Product 1

HCID 54711095HCID 54711095, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Cyclisation of a 60:40 mixture of the ethyl and methyl esters of 2-(N-n-propyl-acetamido) cyclohex-1-ene-1-carboxylic acid (34.82 g; 0.141 mole) as described in Example 8 afforded the title product as a white crystalline solid, m.p. (EtOH) 277° -278° C

Sources & evidence

ORD record
ord-91c21da744164b69825372e8152d56f9
Source dataset
uspto-grants-1977_06
Patent number
US04031099

Reaction notes

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