Morpholine → HCID 20309613, compound

HRID 437379Notes

Reaction equation

HRID 437379 reaction equation
[NH2:1][C:2]1[C:3]([I:18])=[C:4]([C:8]([I:17])=[C:9]([N:12]([CH3:16])[C:13](=[O:15])[CH3:14])[C:10]=1[I:11])[C:5]([OH:7])=O.[NH:19]1[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1>>[NH2:1][C:2]1[C:3]([I:18])=[C:4]([C:8]([I:17])=[C:9]([N:12]([CH3:16])[C:13](=[O:15])[CH3:14])[C:10]=1[I:11])[C:5]([N:19]1[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1)=[O:7]

Participants

3

Reactant 2

HCID 8083MorpholineHCID 203096821949-42-4

Product 1

HCID 20309613HCID 20309613, compound

Procedure

4-[3-Amino-2,4,6-triiodo-5-(N-methylacetamido)benzoyl]morpholine [C; R° is CH3CON(CH3), Q is H, Z is morpholino] was prepared from the acid chloride of 3-amino-5-(N-methylacetamido)-2,4,6-triiodobenzoic acid and morpholine according to the procedure described in Example 45, part (a). The product obtained was used directly in the procedure described in part (b) below.

Workup

  1. customThe product obtained

Sources & evidence

ORD record
ord-5ab56a55a08641d59e5617a967bea5e4
Source dataset
uspto-grants-1977_06
Patent number
US04031088

Reaction notes

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