Benzamide, o-butoxy- → 5-Chloro-2-ethoxybenzamidine hydrochloride

HRID 437424Notes

Reaction equation

HRID 437424 reaction equation
C(OC1C=CC=CC=1C([NH2:10])=O)CCC.[Cl:15][C:16]1[CH:17]=[CH:18][C:19]([O:25][CH2:26][CH3:27])=[C:20]([CH:24]=1)[C:21]([NH2:23])=O>>[ClH:15].[Cl:15][C:16]1[CH:17]=[CH:18][C:19]([O:25][CH2:26][CH3:27])=[C:20]([CH:24]=1)[C:21]([NH2:10])=[NH:23]

Participants

3

Reactant 2

HCID 43269Benzamide, o-butoxy-HCID 203602935-Chloro-2-ethoxybenzamide

Product 1

HCID 203602915-Chloro-2-ethoxybenzamidine hydrochloride

Procedure

If the procedure of Preparation 10 is repeated with the 2-n-butoxybenzamide used therein replaced by an equimolar amount of 5-chloro-2-ethoxybenzamide, there is produced the title product, m.p. 227° with decomposition.

Workup

  1. customIf the procedure of Preparation 10

Sources & evidence

ORD record
ord-6a49a11562214cb5b720a119239f520f
Source dataset
uspto-grants-1977_06
Patent number
US04031093

Reaction notes

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