HCID 12535807, compound → HCID 12535822, compound

HRID 437442Notes

Reaction equation

HRID 437442 reaction equation
Cl.[CH3:2][O:3][C:4]1[CH:5]=[CH:6][C:7]([O:13][CH2:14][CH2:15][CH3:16])=[C:8]([CH:12]=1)[C:9]([NH2:11])=[NH:10].[O:17]=[C:18]1NC(C2C=CC=CC=2OCC=C)=N[CH:20]=[C:19]1[C:34]([O:36][CH2:37][CH3:38])=[O:35]>>[O:17]=[C:18]1[NH:11][C:9]([C:8]2[CH:12]=[C:4]([O:3][CH3:2])[CH:5]=[CH:6][C:7]=2[O:13][CH2:14][CH2:15][CH3:16])=[N:10][CH:20]=[C:19]1[C:34]([O:36][CH2:37][CH3:38])=[O:35]

Participants

3

Reactant 2

HCID 12535807HCID 12535807, compoundHCID 20360290HCID 20360290, compound

Product 1

HCID 12535822HCID 12535822, compound

Procedure

The title compound was prepared from 5-methoxy-2-n-propoxybenzamidine hydrochloride in a manner similar to that described for the preparation of ethyl 1,6-dihydro-6-oxo-2-(2-allyloxyphenyl)pyrimidine-5-carboxylate in Example 8. The product had m.p. 124°-126°.

Sources & evidence

ORD record
ord-7c57dbc4baea4f839d99b92be6b33fe6
Source dataset
uspto-grants-1977_06
Patent number
US04031093

Reaction notes

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