Phosphorus sulfide (P2S5) → 8-Quinolinecarbothioamide, 2-(1,1-dimethylethyl)-5,6,7,8-tetrahydro-

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Reaction Steps

The title compound was prepared from 2-t-butyl-5,6,7,8-tetrahydroquinoline-8-carboxamide (4 g.) and P2S5 (3 g.) as described in Example 8 and was isolated as creamy needles after recrystallisation from n-hexane m.p. 126° C (650 mgs.). Found: C, 68.18; H, 8.25; N, 11.14%. C14H20N2S requires C,67.70; H, 8.12; N, 11.23%.

Provenance & Evidence