Cyclohexyl isothiocyanate → HCID 21427816, compound

HRID 437510Notes

Reaction equation

HRID 437510 reaction equation
[CH:1]([NH:3][NH:4][C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[CH:7][CH:6]=1)=[O:2].[CH:12]1([N:18]=[C:19]=[S:20])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1>>[CH:12]1([NH:18][C:19](=[S:20])[NH:11][C:8]2[CH:9]=[CH:10][C:5]([NH:4][NH:3][CH:1]=[O:2])=[CH:6][CH:7]=2)[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1

Participants

3

Reactant 2

HCID 14289Cyclohexyl isothiocyanateHCID 113189Hydrazinecarboxaldehyde, 2-(4-aminophenyl)-

Product 1

HCID 21427816HCID 21427816, compound

Procedure

Procedure (12.) was employed with 1-formyl-2-(4-aminophenyl)hydrazine (7.5 g, 0.05 mole) and cyclohexyl isothiocyanate 7.1 g, 0.05 mole). Yield 9.6 g (66%), m.p. 158°-160° C.

Sources & evidence

ORD record
ord-d848c2c85e6240d58e07903269c9b3ec
Source dataset
uspto-grants-1977_06
Patent number
US04031127

Reaction notes

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