Benzyl Isothiocyanate → HCID 21427819, compound

Participants

Reaction Steps

1-Formyl-2-(4-aminophenyl)hydrazine (1.51 g, 0.01 mole) and benzyl isothiocyanate (1.49 g, p.01 mole) were mixed in ethanol (30 ml) and the mixture was refluxed for 20 minutes. The product separated from solution as a white solid. The reaction mixture was chilled in ice and the solid was collected by filtration. The product was washed thoroughly with ether and then was dried. Yield 2.5 g (83%), m.p. 152°-154° C.

Provenance & Evidence