Ammonia → HCID 21428510, compound

HRID 437529Notes

Reaction equation

HRID 437529 reaction equation
Cl.[NH2:2][C:3]1[CH:8]=[C:7]([OH:9])[C:6]([Cl:10])=[CH:5][C:4]=1[CH3:11].N>O>[NH2:2][C:3]1[CH:8]=[C:7]([OH:9])[C:6]([Cl:10])=[CH:5][C:4]=1[CH3:11]

Participants

4

Reactant 2

HCID 222AmmoniaHCID 21428511HCID 21428511, compound

Product 1

HCID 21428510HCID 21428510, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The 2-amino-4-hydroxy-5-chloro toluene hydrochloride thus obtained is dissolved in water. The solution is alkalized with ammonia and drying yields 33.8 g of 2-amino-4-hydroxy-5-chloro toluene, which after recrystallization in benzene, melts at 144.5° C.

Workup

  1. customdrying

Sources & evidence

ORD record
ord-3af1062410aa461d80dbe97caf4d592a
Source dataset
uspto-grants-1977_06
Patent number
US04031160

Reaction notes

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