Hydrogen Sulfide → HCID 21428544, compound

Participants

Reaction Steps

To a cold solution of 3-(2,4,5-trimethylanilino)propionitrile (18.9 g.) in dimethylaminoethanol (40 g.) is added hydrogen sulfide (3.5 g.). After three days at room temperature, the mixture is poured on ice and the resulting solid is collected by filtration and recrystallized from benzene to afford 14 g. of 3-(2,4,5-trimethylolanilino)thiopropionamide; m. p. 109.5°-111° C.

Provenance & Evidence