HCID 68121037, compound → HCID 21429284, compound

Participants

Reaction Steps

A solution of 10 g. (0.037 mole) of 6-chloro-N,N-dimethyl-3-phenyl-3-hexenylamine hydrochloride in 150 ml. of 95% ethanol was hydrogenated using palladium on carbon catalyst. Hydrogenation was complete after 15 minutes at room temperature. The catalyst was removed by filtration and the filtrate was evaporated to a solid. Recrystallization of the solid from isobutyl methyl ketone gave 7 g. (70%) of a hygroscopic solid.

Provenance & Evidence