HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 5-(Prop-2-en-1-yl)thiopyrano[3,2-b]indol-4(5H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Thiopyrano[3,2-b]indol-4(5H)-one | HCID 20326608 | — |
| Product | 5-(Prop-2-en-1-yl)thiopyrano[3,2-b]indol-4(5H)-one | HCID 20326623 | — |
Reaction Steps
By the same method as described in Example 7, 4.8 g of thiopyrano [3,2-b]-indol-4(5H)-one is alkylated with allyl bromide to give 3.9 g of product, mp 67°-68° C., after recrystallization from methylene chloride-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032537 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-a64f357beaaf4a8c88a112df3741d4e4 |
| Source note | uspto-grants-1977_06 |