HuagongsheHuagongshe Chemistry Print Report · For research reference only
Homoveratrylamine → HCID 20371579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Homoveratrylamine | HCID 8421 | — |
| Reactant | HCID 20371574 | HCID 20371574 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20371579 | HCID 20371579 | 47.2% |
Reaction Steps
A solution of 5 g of α-chloro-2-benzyloxyacetophenone in 15 ml of methylene chloride is added dropwise to 10.5 g of 3,4-dimethoxyphenethylamine. The mixture is refluxed for one hour. Then, the mixture is treated in the same manner as described in Example 1-(a). 4 g of α-(3,4-dimethoxyphenethylamino)-2-benzyloxyacetophenone hydrochloride are obtained. M.p. 177° -180° C. (recrystallized from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032575 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-4e50c33f9e6642188747308cb0191b47 |
| Source note | uspto-grants-1977_06 |