HRID437945

反应详情

EQUATION

反应方程式

HRID 437945 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Hydrogen was added with stirring for 2 hours to a mixture of 25 g of ethyl 5-(2-propyl-5-thiazolyl)-2,4-pentadienoate, 250 ml of ethanol and 12.5 g of activated carbon containing 10% palladium and the mixture was filtered. The fiter was washed with ethanol and the filtrate was evaporated to dryness under reduced pressure to obtain 23 g of raw ethyl 2-propyl- 5-thiazolepentanoate.

WORKUP

后处理

  1. filtrationthe mixture was filtered
  2. washThe fiter was washed with ethanol
  3. customthe filtrate was evaporated to dryness under reduced pressure