HRID437945
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Hydrogen was added with stirring for 2 hours to a mixture of 25 g of ethyl 5-(2-propyl-5-thiazolyl)-2,4-pentadienoate, 250 ml of ethanol and 12.5 g of activated carbon containing 10% palladium and the mixture was filtered. The fiter was washed with ethanol and the filtrate was evaporated to dryness under reduced pressure to obtain 23 g of raw ethyl 2-propyl- 5-thiazolepentanoate.
WORKUP
后处理
- filtrationthe mixture was filtered
- washThe fiter was washed with ethanol
- customthe filtrate was evaporated to dryness under reduced pressure