HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroaniline → HCID 178467262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroaniline | HCID 7240 | — |
| Reactant | 3,5-Diacetyl-2,6-dihydroxy-4h-pyran-4-one | HCID 135465969 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178467262 | HCID 178467262 | — |
Reaction Steps
o-Chloroaniline (2.55 g., 0.02 m.) is added to 4.24 g. (0.02 m.) of 3,5-diacetyl-4,6-dihydroxy-2H-pyran-2-one in 150 ml. of methanol and the mixture is refluxed overnight. The reaction mixture is concentrated, cooled and filtered to give 5-acetyl-3-[1-(o-chlorophenylamino)ethylidene]-4-hydroxy-2H-pyran-2,6(3H)-dione, m.p. 143°-145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032652 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-9cde278dbf644e908d76a66960ba9c0e |
| Source note | uspto-grants-1977_06 |