HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Lysine → HCID 22798342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Lysine | HCID 5962 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Catalyst | Nickel | HCID 935 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22798342 | HCID 22798342 | — |
Reaction Steps
The starting materials were D-glucose and L-(+)-lysine in a molar ratio 2:1. The reductive amination took place using Raney nickel or palladium/activated carbon (10%) as a catalyst and heating for 2 hours to 50° C. and 4 hours to 70° C., a yellowish resin-like product being obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032676 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-36c2af6699684dbcaf00567876e52cd3 |
| Source note | uspto-grants-1977_06 |