HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citrulline → N-(2,3,4,5-tetrahydroxy-pentyl)-L-(+)-citrulline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citrulline | HCID 9750 | — |
| Reactant | Aldehydo-D-ribose | HCID 5311110 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | N-(2,3,4,5-tetrahydroxy-pentyl)-L-(+)-citrulline | HCID 54340382 | — |
Reaction Steps
The product was made from D-ribose and L-(+)-citrulline using Raney nickel as a catalyst and heating for 2 hours to 50° C. and for 4 hours to 70° C. The product obtained had a melting point of 172° to 175° C. (decomposition) and an RF -value of 0.52 (determined as indicated under Example T).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032676 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-83b4416ca09743c682d22a1ff915884c |
| Source note | uspto-grants-1977_06 |