HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54122811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2(5H)-Thiophenone | HCID 137898 | — |
| Reactant | HCID 54090976 | HCID 54090976 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54122811 | HCID 54122811 | — |
Reaction Steps
A mixture of 20.0 g (0.2 mole) of 3-thiolen-2-one [R. T. Hawkins, J. Heterocyclic Chem., 11 291-4 (1974)] 65.5 g (0.2 mole) of 1-bromo-9,12,15-octadecatriene, and 4.8 g (0.2 mole) of sodium hydride in benzene is refluxed with stirring for 24 hours after which the solvent is removed, and the product distilled to give 2-(9,12,15-octadecatrienyloxy)thiophene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032647 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-47088685bb484ca6ae5d8cf5de83a863 |
| Source note | uspto-grants-1977_06 |