HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → Ethaboxam
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 54448843 | HCID 54448843 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Ethaboxam | HCID 11174640 | 70% |
Reaction Steps
1.0g of 2-bromo-4-ethyl-thiazole-5-carboxylic acid (cyano-thiophen-2-yl-methyl)-amide, 0.40ml of triethylamine and 0.55ml of ethylamine were added to 10ml of tetrahydrofuran. The reaction mixture was stirred under reflux for 4 hours and then treated according to the same procedure as EXAMPLE 10 to obtain 0.63g (Yield 70%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514643 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-a92cec7a1da84bd5a46e800b598f15e7 |
| Source note | uspto-grants-1996_05 |