3-Isocyanatopyridine → HCID 22411373, compound

HRID 439342Notes

Reaction equation

HRID 439342 reaction equation
[C:1]([C:3]1[CH:12]=[C:11]2[C:6]([C:7]([CH3:23])([CH3:22])[CH2:8][CH2:9][N:10]2[C:13]([NH:15][C:16]2[CH:21]=C[CH:19]=[CH:18][CH:17]=2)=[O:14])=[CH:5][CH:4]=1)#[N:2].[N:24]1C=CC=C(N=C=O)C=1>>[C:1]([C:3]1[CH:12]=[C:11]2[C:6]([C:7]([CH3:22])([CH3:23])[CH2:8][CH2:9][N:10]2[C:13]([NH:15][C:16]2[CH:21]=[N:24][CH:19]=[CH:18][CH:17]=2)=[O:14])=[CH:5][CH:4]=1)#[N:2]

Participants

3

Reactant 2

HCID 27604933-IsocyanatopyridineHCID 9948447HCID 9948447, compound2×

Product 1

HCID 22411373HCID 22411373, compound

Procedure

The title compound was prepared from 7-cyano-3,4-dihydro-4,4-dimethyl-1(2H)-quinoline (compound of example 1, part J) and 3-pyridylisocyanate by the same method as described in example 1, part K. The product was obtained as a colorless powder; m.p. 183°-185° C.

Workup

  1. customThe product was obtained as a colorless powder

Sources & evidence

ORD record
ord-56ec097215a34ff79c57533c9e2f7b2f
Source dataset
uspto-grants-1996_05
Patent number
US05514690

Reaction notes

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