HCID 22411376, compound → HCID 15453193, compound

HRID 439346Notes

Reaction equation

HRID 439346 reaction equation
N[C:2]1[CH:3]=[C:4]([S:8]([NH:11][C:12]2[O:16][N:15]=[C:14]([CH3:17])[C:13]=2[Br:18])(=[O:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.NC1C=CC=CC=1S(N[C:30]1[O:34]N=C(C)C=1Br)(=O)=O.[N+](C1C=CC=CC=1S(N[C:50]1[O:54]N=C(C)C=1Br)(=O)=O)([O-])=O>>[CH3:50][O:54][C:5]1[CH:6]=[CH:7][C:2]([O:34][CH3:30])=[CH:3][C:4]=1[S:8]([NH:11][C:12]1[O:16][N:15]=[C:14]([CH3:17])[C:13]=1[Br:18])(=[O:10])=[O:9]

Participants

4

Reactant 3

HCID 22411376HCID 22411376, compoundHCID 22411377HCID 22411377, compoundHCID 22411381HCID 22411381, compound

Product 1

HCID 15453193HCID 15453193, compound

Procedure

3-Amino-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide and 2-amino-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide can be prepared by hydrogenation of corresponding nitro-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide, which is prepared as described above.

Workup

  1. customis prepared

Sources & evidence

ORD record
ord-264d23e36313418596aae2a3bc577c56
Source dataset
uspto-grants-1996_05
Patent number
US05514691

Reaction notes

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