HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxybenzenesulfonyl chloride → HCID 15453193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxybenzenesulfonyl chloride | HCID 137025 | — |
| Reactant | 4-Bromo-3-methylisoxazol-5-amine | HCID 10487519 | — |
| Product | HCID 15453193 | HCID 15453193 | 58% |
Reaction Steps
2,5-Dimethoxy-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide was prepared from 5-amino-4-bromo-3-methylisoxazole and 2,5-dimethoxybenzenesulfonyl chloride according to the procedures described in Example 5. The crude product was purified by recrystallization from ethyl acetate/hexanes to give a crystalline solid, m.p. 118°-120° C. yield 58%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514691 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-7af85501be9d4c9c9a84f2f6a27d96c8 |
| Source note | uspto-grants-1996_05 |