HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dansyl chloride → HCID 9909467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dansyl chloride | HCID 11801 | — |
| Reactant | 4-Bromo-3-methylisoxazol-5-amine | HCID 10487519 | — |
| Product | HCID 9909467 | HCID 9909467 | 68% |
Reaction Steps
5-Dimethylamino-N-(4-bromo-3-methyl-5-isoxazolyl)-1-naphthalenesulfonamide was prepared from 5-amino-4-bromo-3-methylisoxazole and 5-dimethylaminonaphthalenesulfonyl chloride according to the procedures described in Example 5. The crude product was purified by recrystallization from ethyl acetate/hexanes to give a crystalline solid, m.p. 87°-89° C., yield 68%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514691 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-630fc198ffac4833a3f5563f7ed53691 |
| Source note | uspto-grants-1996_05 |