HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-chlorophenyl)-2-cyanoacetamide → HCID 54449681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-chlorophenyl)-2-cyanoacetamide | HCID 679494 | — |
| Reactant | 4,5-Dihydroxy-2-nitrobenzaldehyde | HCID 3782344 | — |
| Product | HCID 54449681 | HCID 54449681 | 28% |
Reaction Steps
The reaction of 4, 5-dihydroxy-2-nitrobenzaldehyde (185 mg, 1.01 mmol) and N-(3-chlorophenyl) cyanoacetamide (197 mg, 1.01 mmol) was effected in the same manner as in Example 1 to give the objective N-(3-chlorophenyl)-2-cyano-3-(4, 5-dihydroxy-2-nitrophenyl)propenamide (100 mg, 28% in yield) as brown powdery crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514711 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-82036408465c4a08adc84b13d945dfb6 |
| Source note | uspto-grants-1996_05 |