HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 439713Generated: October 27, 2026
Acetic Anhydride → HCID 53661794, compound
https://huagongshe.com/reaction/439713
Participants
| Role | Name | HCID | Charge |
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| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 22402967 | HCID 22402967 | — |
| Product | HCID 53661794 | HCID 53661794 | 91.1% |
Reaction Steps
A mixture of the 1-benzyl-2-methyl-4,5-benzimidazoledicarboxylic acid (4.40 g, 14.2 mmol) and acetic anhydride is stirred for 5 hours at reflux temperature, cooled to 0° C. and filtered to give the title product as a pale yellow solid (3.78 g, 91.1%), identified by 1HNMR spectrography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05516751 |
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| Source dataset | uspto-grants-1996_05 |
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| ORD ID | ord-759bc2bac59b4325b88af0c902698879 |
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| Source note | uspto-grants-1996_05 |
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