HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(5-Benzyloxypentyl)(1-hexenyl)benzene → 5-(3-Hexylphenyl)-pentanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(5-Benzyloxypentyl)(1-hexenyl)benzene | HCID 53925500 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-(3-Hexylphenyl)-pentanol | HCID 22407876 | — |
Reaction Steps
A solution of 840 mgs of 3-(5-benzyloxypentyl)-1-(1-hexenyl)benzene in 25 mls of methanol is hydrogenated over 5% palladium on carbon and then filtered through celite, concentrated, and chromatographed over silica gel (3:2 ether:hexane) to yield pure 5-(3-hexylphenyl)-pentanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516767 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-fd56fa22d76b409eb0ebbbfb54927de7 |
| Source note | uspto-grants-1996_05 |