HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 86749480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 86749481 | HCID 86749481 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Product | HCID 86749480 | HCID 86749480 | — |
Reaction Steps
Next, 6.17 g, that is, 17 mmol methyl 2,3,4-tri-O-acetylglucopyranuronosyl azide was added to 50 ml of dry tetrahydrofuran containing 400 mg of PtO2. The mixture was shaken under 40 psi of hydrogen for 2 hours, filtered, concentrated to dryness, to produce methyl 2,3,4-tri-O-acetylglucopyranuronosyl amine. ##STR8## Preparation of methyl 2,3,4-tri-O-acetylglucopyranuronosyl retinamide
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516792 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-163d2619e1534ab58d69afd44f7a2f2f |
| Source note | uspto-grants-1996_05 |