HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Benzoic acid, 4-ethyl-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Ethylbenzoic Acid | HCID 12086 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Benzoic acid, 4-ethyl-, methyl ester | HCID 23827 | — |
Reaction Steps
A mixture of 4-ethylbenzoic acid (5.12 g), thionyl chloride (3.0 ml) and methanol (150 ml) was heated and refluxed. After 3 hours, the mixture was concentrated under reduced pressure to give methyl 4-ethylbenzoate (5.59 g). this product was used in the subsequent step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516777 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-cfb03ca1633a47faa484d1cc6cde5262 |
| Source note | uspto-grants-1996_05 |