HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxyphthalimide → HCID 178454092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | HCID 178454090 | HCID 178454090 | — |
| Product | HCID 178454092 | HCID 178454092 | — |
Reaction Steps
Analogously to Example 6a, starting from 5.6 g (0.02782 mol) of trans-3-(N-BOC-amino)-cyclobutanemethanol, 4.54 g (0.02783 mol) of N-hydroxyphthalimide, 7.3 g (0.02783 mol) of triphenylphosphine and 5.12 ml (0.0306 mol) of diethyl azodicarboxylate (93%), the title compound is obtained, m.p. 120°-122° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516806 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-0691530c4ab9456ca847b6a0954b0e10 |
| Source note | uspto-grants-1996_05 |