HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21837097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
| Reactant | HCID 21836981 | HCID 21836981 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21837097 | HCID 21837097 | — |
Reaction Steps
As described for Example 125 a mixture of 1.0 mmol of 7-methoxy-10,11-dihydro-5H-imidazo[2,1-c][1,4]-benzodiazepine, 1.1 mmol of 4-[(2-methylbenzoyl)amino]-benzoyl chloride and 1.5 mmol of triethylamine in 10 ml of dichloromethane is stirred for 3 hours at room temperature and worked up to give the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516774 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-102c24c9b7d7427da15aef15f95f5a71 |
| Source note | uspto-grants-1996_05 |