HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-ethyl-9H-carbazole-3-carbaldehyde → 1-(N-Ethylcarbazol-3-yl)-2-[4-(3-tetrahydropyranyloxy)-1-propylsulfonylphenyl]ethene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-ethyl-9H-carbazole-3-carbaldehyde | HCID 82055 | — |
| Reactant | Dichloromethane ethylacetate | HCID 21226138 | — |
| Reactant | 3-(4-Methylphenyl)sulfonyl-1-tetrahydropyranyloxypropane | HCID 22076178 | — |
| Reactant | 4-Dimethylamino-4'-[(3-tetrahydropyranoyloxy)-1-propylsulfonyl]stilbene | HCID 86749484 | — |
| Product | 1-(N-Ethylcarbazol-3-yl)-2-[4-(3-tetrahydropyranyloxy)-1-propylsulfonylphenyl]ethene | HCID 67772200 | — |
Reaction Steps
As in Example 3a 2.98 g (10 mmol) of 2a and 2.68 g (12 mmol) of N-ethylcarbazole-3-carboxaldehyde give, after column chromatography. [silica gel; dichloromethane/ethyl acetate mixtures], 1.56 g (31%) of yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05517350 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-a5e3cf8503d04f2b85406ce3dac2fac4 |
| Source note | uspto-grants-1996_05 |