HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexadecane → HCID 22410881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexadecane | HCID 8213 | — |
| Reactant | Sodium p-toluenesulfinate | HCID 2723791 | — |
| Reactant | Dichloromethane ethylacetate | HCID 21226138 | — |
| Product | HCID 22410881 | HCID 22410881 | 94% |
Reaction Steps
As in Example 2a, 9.15 g (30 mmol) of 1-bromohexadecane and 5.88 g (33 mmol) of sodium p-toluenesulfinate (anhydrous) are reacted. After chromatography on a short silica gel column (dichloromethane/ethyl acetate 10:1) 10.7 g (94%) of 5a are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05517350 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-b8caef18c452483f952103842cf5d708 |
| Source note | uspto-grants-1996_05 |