demeclocycline → HCID 131719400, compound

Participants

Reaction Steps

One point five (1.5) g (0.01 mole) of DMcT monomer powder were dissolved in 5 g of NMP to obtain a yellowish transparent viscous DMcT-NMP solution. To this solution, 2.5 g (0.015 mole) of polyaniline powder in a de-doped reduced state ("ANILEAD" available from Nitto Denko Corp., Japan) were added and the combined solution was then heated. at 80° C. in a sealed container, whose inner atmosphere was substituted by an inert gas, to obtain a black purple liquid.

Provenance & Evidence